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OfflineYrat
Happy Planting
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Registered: 04/20/08
Posts: 886
Last seen: 11 years, 1 month
Re: Lets make Hexane Hash!! [Re: captain.koons]
    #67499 - 06/27/08 01:07 PM (16 years, 9 months ago)

Quote:

captain.koons said:
butane converts inactive alkloids into active ones.





Quote:

captain.koons said: a big claim




please explain to me how an inert hydrocarbon can possibly react in any way with an "inactive" alkaloid.


coda, cool process, thanks for the photos!  but do u mind telling me WTF you had in that jar that requires the sticker seen in the second pic. :eek:


--------------------
"Prohibition will work great injury to the cause of temperance. It is a species of intemperance within itself, for it goes beyond the bounds of reason in that it attempts to control a man's appetite by legislation, and makes a crime out of things that are not crimes. A Prohibition law strikes a blow at the very principles upon which our government was founded." - Abraham Lincoln


"There are a thousand hacking at the branches of evil
to one who is striking at the root"
~ Henry D. Thoreau
Strike The Root
                                                                                      :gethigh:

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OfflineYrat
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Registered: 04/20/08
Posts: 886
Last seen: 11 years, 1 month
Re: Lets make Hexane Hash!! **COMPLETED** [Re: captain.koons]
    #79653 - 07/11/08 08:31 PM (16 years, 8 months ago)

:lol:


--------------------
"Prohibition will work great injury to the cause of temperance. It is a species of intemperance within itself, for it goes beyond the bounds of reason in that it attempts to control a man's appetite by legislation, and makes a crime out of things that are not crimes. A Prohibition law strikes a blow at the very principles upon which our government was founded." - Abraham Lincoln


"There are a thousand hacking at the branches of evil
to one who is striking at the root"
~ Henry D. Thoreau
Strike The Root
                                                                                      :gethigh:

Extras: Unfilter Print Post Top
OfflineYrat
Happy Planting
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Registered: 04/20/08
Posts: 886
Last seen: 11 years, 1 month
Re: Lets make Hexane Hash!! [Re: tg105]
    #226639 - 05/15/09 10:19 AM (15 years, 10 months ago)

i am planning on possibly doing a hexane pull this weekend, and have a quick question.  if the oil is warm enough, is the viscosity still too great to transfer with, say, a Pasteur pipette?  i may possibly rotovap the hexane to finish the process in minutes, and am wondering about the possibility of removing the oil from something like a round bottom flask.


--------------------
"Prohibition will work great injury to the cause of temperance. It is a species of intemperance within itself, for it goes beyond the bounds of reason in that it attempts to control a man's appetite by legislation, and makes a crime out of things that are not crimes. A Prohibition law strikes a blow at the very principles upon which our government was founded." - Abraham Lincoln


"There are a thousand hacking at the branches of evil
to one who is striking at the root"
~ Henry D. Thoreau
Strike The Root
                                                                                      :gethigh:

Extras: Unfilter Print Post Top
OfflineYrat
Happy Planting
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Registered: 04/20/08
Posts: 886
Last seen: 11 years, 1 month
Re: Lets make Hexane Hash!! [Re: Dr. Penguin]
    #228515 - 05/20/09 08:16 AM (15 years, 10 months ago)

hmmm.... that's what i was afraid of.

i suppose one could rotovap down most, if not all, of the hexane, and then redissolve in a much smaller amount to transfer the oil out into a more suitable evaporation dish.  this would definitely speed up the evaporation process significantly, i know that i could do something like a liter of hexane in under an hour with the rotovap, not to mention capturing and recycling it.


--------------------
"Prohibition will work great injury to the cause of temperance. It is a species of intemperance within itself, for it goes beyond the bounds of reason in that it attempts to control a man's appetite by legislation, and makes a crime out of things that are not crimes. A Prohibition law strikes a blow at the very principles upon which our government was founded." - Abraham Lincoln


"There are a thousand hacking at the branches of evil
to one who is striking at the root"
~ Henry D. Thoreau
Strike The Root
                                                                                      :gethigh:

Extras: Unfilter Print Post Top
OfflineYrat
Happy Planting
 User Gallery

Registered: 04/20/08
Posts: 886
Last seen: 11 years, 1 month
Re: Lets make Hexane Hash!! [Re: coda]
    #237873 - 06/09/09 05:36 AM (15 years, 9 months ago)

well, it turns out the person with a large amount of trim and already gone through it for ice hash :mad2:

i just like the rotovap idea for it's speed, ease, and re-capture of the hexane for repeat use.  hopefully i'll be able to try it out soon.  i'll make sure to post my results here and let you guys know.  i'm thinking i will get the volume of the hexane down to a very small amount, just enough to keep the oils soluble and avoid the viscosity, and then transfer this right out into a collection plate, and evap from there, maybe on a warm hot plate.


--------------------
"Prohibition will work great injury to the cause of temperance. It is a species of intemperance within itself, for it goes beyond the bounds of reason in that it attempts to control a man's appetite by legislation, and makes a crime out of things that are not crimes. A Prohibition law strikes a blow at the very principles upon which our government was founded." - Abraham Lincoln


"There are a thousand hacking at the branches of evil
to one who is striking at the root"
~ Henry D. Thoreau
Strike The Root
                                                                                      :gethigh:

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